Issue 12, 2015
From the journal:

Analyst

Ultrafast high-resolution magic-angle-spinning NMR spectroscopy†

Marion André,a   Martial Piotto,bc   Stefano Caldarelliad  and  Jean-Nicolas Dumez*a  

* Corresponding authors

a Institut de Chimie des Substances Naturelles, CNRS UPR 2301, Avenue de la Terrasse, 91190 Gif-sur-Yvette, France
E-mail: jeannicolas.dumez@cnrs.fr

b Bruker Biospin, Laboratoire d'applications RMN, 34 rue de l'industrie, 67166 Wissembourg, France

c Strasbourg University, IMIS/ICube Laboratory, 67000 Strasbourg, France

d Aix Marseille Université, Centrale Marseille, CNRS, iSm2 UMR 7313, 13397 Marseille, France

Abstract

We demonstrate the acquisition of ultrafast 2D NMR spectra of semi-solid samples, with a high-resolution magic-angle-spinning setup. Using a recent double-quantum NMR pulse sequence in optimised synchronisation conditions, high-quality 2D spectra can be recorded for a sample under magic-angle spinning. An illustration is given with a semi-solid sample of banana pulp.

Graphical abstract: Ultrafast high-resolution magic-angle-spinning NMR spectroscopy

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Article information

DOI
https://doi.org/10.1039/C5AN00653H
Article type
Communication
Submitted
03 Apr 2015
Accepted
30 Apr 2015
First published
30 Apr 2015

Analyst, 2015,140, 3942-3946

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Ultrafast high-resolution magic-angle-spinning NMR spectroscopy

M. André, M. Piotto, S. Caldarelli and J. Dumez, Analyst, 2015, 140, 3942 DOI: 10.1039/C5AN00653H

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