Issue 3, 2009

High temperature liquid chromatography with monolithic capillary columns and pure watereluent

Abstract

Use of an organic polymeric monolithic stationary phase for high temperature liquid chromatography (HTLC) with a pure water eluent is demonstrated for the first time. Separations of n-alcohols at temperatures exceeding 200 °C were achieved with no statistically significant reduction in chromatographic performance evident after continuous operation for 1000 column volumes above 200 °C.

Graphical abstract: High temperature liquid chromatography with monolithic capillary columns and pure water eluent

Article information

Article type
Communication
Submitted
11 Sep 2008
Accepted
10 Dec 2008
First published
24 Dec 2008

Analyst, 2009,134, 440-442

High temperature liquid chromatography with monolithic capillary columns and pure water eluent

T. J. Causon, R. A. Shellie and E. F. Hilder, Analyst, 2009, 134, 440 DOI: 10.1039/B815886J

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