A nickel-catalyzed cross-coupling reaction of o-carboranyl with alkenyl bromides has been developed, affording a series of 1,2-dialkenylated o-carboranes with a broad substrate scope. This reaction provides an efficient and concise strategy for C,C′-dialkenylation of o-carboranes and supplements the transition-metal catalyzed cage B–H functionalization systems.
Q. Zhuo, J. Zhang and Z. Xie, Dalton Trans., 2025, 54, 17430 DOI: 10.1039/D5DT02451J
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