Issue 39, 2023
From the journal:

Organic & Biomolecular Chemistry

Confirmation of the structure of (±)-preisomide by total synthesis†

Hong Kang Teo,a   Patcharaporn Sae-Laoa  and  Roderick W. Bates ORCID logo *a  

* Corresponding authors

a School of Chemistry, Chemical Engineering and Biotechnology, Nanyang Technological University, 21 Nanyang Link, Singapore 637371
E-mail: Roderick@ntu.edu.sg

Abstract

The structure of preisomide has been confirmed by total synthesis involving chemoselective oxazine formation and vinyl iodide carbonylation in six steps (longest linear sequence) and 23% overall yield.

Graphical abstract: Confirmation of the structure of (±)-preisomide by total synthesis

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Article information

DOI
https://doi.org/10.1039/D3OB01250F
Article type
Paper
Submitted
08 Aug 2023
Accepted
14 Sep 2023
First published
26 Sep 2023

Org. Biomol. Chem., 2023,21, 7954-7959

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Confirmation of the structure of (±)-preisomide by total synthesis

H. K. Teo, P. Sae-Lao and R. W. Bates, Org. Biomol. Chem., 2023, 21, 7954 DOI: 10.1039/D3OB01250F

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