SCHEDULED MAINTENANCE
The synthesis of difluoromethyl-containing compounds exploiting the deoxofluorination reaction of aromatic aldehydes using XtalFluor-E is described. This transformation occurs at room temperature under highly concentrated conditions, i.e., with no added solvent. A wide range of difluoromethyl-containing compounds was obtained in 21 to 87% isolated yields.
O. Thibeault, M. Ouellet-Du Berger, M. Gonay and J. Paquin, Org. Biomol. Chem., 2023, 21, 6115 DOI: 10.1039/D3OB00859B
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