Issue 19, 2023
From the journal:

Organic & Biomolecular Chemistry

Microwave-promoted radical addition/cyclization of biaryl vinyl ketones with diacyl peroxides in water under metal-free conditions†

Xingyu Yang,ab   Gan Zhang,b   Jingwen Zhou,b   Chao Zhou,*b   Lei Wang ORCID logo c  and  Pinhua Li ORCID logo *a  

* Corresponding authors

a College of Chemical and Environmental Engineering, Anhui Polytechnic University, Wuhu, Anhui 241000, P. R. China
E-mail: pphuali@126.com

b Key Laboratory of Green and Precise Synthetic Chemistry and Applications, Ministry of Education, College of Chemistry and Materials Science, Huaibei Normal University, Huaibei, Anhui 235000, P. R. China
E-mail: zhouch110@163.com

c Advanced Research Institute and Department of Chemistry, Taizhou University, Taizhou, Zhejiang 318000, P. R. China

Abstract

This communication reports an efficient microwave-promoted radical addition/cyclization reaction of biaryl vinyl ketones with diacyl peroxides in water under metal-free conditions. A series of 10-methyl-10-benzyl(alkyl)phenanthren-9(10H)-ones were obtained in high yields with good functional group tolerance.

Graphical abstract: Microwave-promoted radical addition/cyclization of biaryl vinyl ketones with diacyl peroxides in water under metal-free conditions

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Article information

DOI
https://doi.org/10.1039/D3OB00115F
Article type
Communication
Submitted
24 Jan 2023
Accepted
20 Apr 2023
First published
21 Apr 2023

Org. Biomol. Chem., 2023,21, 4018-4021

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Microwave-promoted radical addition/cyclization of biaryl vinyl ketones with diacyl peroxides in water under metal-free conditions

X. Yang, G. Zhang, J. Zhou, C. Zhou, L. Wang and P. Li, Org. Biomol. Chem., 2023, 21, 4018 DOI: 10.1039/D3OB00115F

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