A free radical nitration of olefins with NaNO2/I2O5

Xuan Huang; Huichao You; Fang Fang; Fan Wang; Zhong-Quan Liu

doi:10.1039/D3CC04275H

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A free radical nitration of olefins with NaNO₂/I₂O₅†

Xuan Huang,^a Huichao You,^a Fang Fang,^a Fan Wang^a and Zhong-Quan Liu

*^a

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* Corresponding authors

^a Jiangsu Collaborative Innovation Center of Chinese Medicinal Resources Industrialization, College of Pharmacy, Nanjing University of Chinese Medicine, Nanjing 210023, P. R. China
E-mail: liuzhq@lzu.edu.cn

Abstract

We demonstrated herein an I₂O₅-mediated radical nitration of olefins with NaNO₂. A variety of (E)-nitroolefins can be synthesized in high yields and chemoselectivity.

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Article information

DOI: https://doi.org/10.1039/D3CC04275H
Article type: Communication
Submitted: 31 Aug 2023
Accepted: 16 Oct 2023
First published: 18 Oct 2023

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Chem. Commun., 2023,59, 13352-13354

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A free radical nitration of olefins with NaNO₂/I₂O₅

X. Huang, H. You, F. Fang, F. Wang and Z. Liu, Chem. Commun., 2023, 59, 13352 DOI: 10.1039/D3CC04275H

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