Synthesis of 1,3-diselenyl-dihydroisobenzofurans via electrochemical radical selenylation with substituted o-divinylbenzenes and diselenides

Ying Wang; Ning Xu; Weiwei Li; Jiaojiao Li; Yijun Huo; Wenrong Zhu; Qiang Liu

doi:10.1039/D2OB00254J

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Synthesis of 1,3-diselenyl-dihydroisobenzofurans via electrochemical radical selenylation with substituted o-divinylbenzenes and diselenides†

Ying Wang,^a Ning Xu,^b Weiwei Li,^a Jiaojiao Li,^a Yijun Huo,^a Wenrong Zhu^a and Qiang Liu

*^a

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* Corresponding authors

^a Jiangsu Key Laboratory of Marine Pharmaceutical Compound Screening, Jiangsu Ocean University; School of Pharmacy, Jiangsu Ocean University, Lianyungang, Jiangsu, China
E-mail: 2020000040@jou.edu.cn

^b School of Metallurgy and Environment, Central South University, Changsha, Hunan, China

Abstract

An efficient electrochemical method for the direct synthesis of complicated 1,3-diselenyl-dihydroisobenzofurans was developed under external oxidant free conditions at room temperature from substituted o-divinylbenzenes and diselenides. A radical mechanism is proposed for this novel and practical transformation.

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DOI: https://doi.org/10.1039/D2OB00254J
Article type: Communication
Submitted: 05 Feb 2022
Accepted: 15 Mar 2022
First published: 16 Mar 2022

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Org. Biomol. Chem., 2022,20, 2813-2817

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Synthesis of 1,3-diselenyl-dihydroisobenzofurans via electrochemical radical selenylation with substituted o-divinylbenzenes and diselenides

Y. Wang, N. Xu, W. Li, J. Li, Y. Huo, W. Zhu and Q. Liu, Org. Biomol. Chem., 2022, 20, 2813 DOI: 10.1039/D2OB00254J

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Organic & Biomolecular Chemistry

Synthesis of 1,3-diselenyl-dihydroisobenzofurans via electrochemical radical selenylation with substituted o-divinylbenzenes and diselenides†

Abstract

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Synthesis of 1,3-diselenyl-dihydroisobenzofurans via electrochemical radical selenylation with substituted o-divinylbenzenes and diselenides

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