High-efficiency and simple synthesis of Ti3C2Tx nanoscrolls by surface energy modulation and cryogenic freezing

Ke Tan; Sen Liu; Yang Liu; Linrui Hou; Changzhou Yuan

doi:10.1039/D2NA00520D

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High-efficiency and simple synthesis of Ti₃C₂T_x nanoscrolls by surface energy modulation and cryogenic freezing†

Ke Tan,‡^a Sen Liu,‡^a Yang Liu,*^a Linrui Hou

*^a and Changzhou Yuan

*^a

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* Corresponding authors

^a School of Material Science & Engineering, University of Jinan, Jinan, P. R. China
E-mail: mse_liuy@ujn.edu.cn, mse_houlr@ujn.edu.cn, mse_yuancz@ujn.edu.cn

Abstract

To alleviate the restacking issue of 2D Ti₃C₂T_x itself, we purposefully explore a simple but efficient method for controllable construction of 1D Ti₃C₂T_x nanoscrolls with a high efficiency of ∼90.5%, with detailed regulation of the feed concentrations and surface energy of Ti₃C₂T_x. The involved transformation mechanism from 2D nanosheets to 1D nanoscrolls is reasonably proposed.

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Article information

DOI: https://doi.org/10.1039/D2NA00520D
Article type: Communication
Submitted: 05 Aug 2022
Accepted: 27 Oct 2022
First published: 27 Oct 2022
This article is Open Access

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Nanoscale Adv., 2022,4, 5253-5256

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High-efficiency and simple synthesis of Ti₃C₂T_x nanoscrolls by surface energy modulation and cryogenic freezing

K. Tan, S. Liu, Y. Liu, L. Hou and C. Yuan, Nanoscale Adv., 2022, 4, 5253 DOI: 10.1039/D2NA00520D

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