Bis(imino)carbazolate lead(II) fluoride and related halides

Peter M. Chapple; Ghanem Hamdoun; Thierry Roisnel; Jean-François Carpentier; Hassan Oulyadi; Yann Sarazin

doi:10.1039/D1DT01615F

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Bis(imino)carbazolate lead(ii) fluoride and related halides†

Peter M. Chapple,

^a Ghanem Hamdoun,^b Thierry Roisnel,

^a Jean-François Carpentier,

^a Hassan Oulyadi

^c and Yann Sarazin

*^a

Author affiliations

* Corresponding authors

^a Univ Rennes, CNRS, ISCR (Institut des Sciences Chimiques de Rennes) – UMR 6226, Rennes F-35000, France
E-mail: yann.sarazin@univ-rennes1.fr
Tel: +33 223-233019

^b Euromed University of Fes (UEMF), Fez, Morocco

^c Normandie Université, UNIROUEN, INSA de Rouen, CNRS, Laboratoire COBRA (UMR 6014 & FR 3038), 76000 Rouen, France

Abstract

The versatility of a bulky bis(imino)carbazolate ligand in lead(II) chemistry is illustrated by the synthesis of a soluble, heteroleptic lead(II) fluoride and several halide (Cl, Br and I), amide and hydrocarbyl congeners. All complexes have been structurally authenticated, and a full set of ²⁰⁷Pb NMR data is discussed.

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Article information

DOI: https://doi.org/10.1039/D1DT01615F
Article type: Communication
Submitted: 18 May 2021
Accepted: 24 May 2021
First published: 04 Jun 2021

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Dalton Trans., 2021,50, 9021-9025

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Bis(imino)carbazolate lead(II) fluoride and related halides

P. M. Chapple, G. Hamdoun, T. Roisnel, J. Carpentier, H. Oulyadi and Y. Sarazin, Dalton Trans., 2021, 50, 9021 DOI: 10.1039/D1DT01615F

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Dalton Transactions

Bis(imino)carbazolate lead(ii) fluoride and related halides†

Abstract

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Bis(imino)carbazolate lead(II) fluoride and related halides

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