The construction of three-dimensional (3D) covalent organic frameworks (COFs), especially fully conjugated 3D COFs, is a long-standing challenge. Herein, we report a saddle-like, π-conjugated cyclooctatetrathiophene (COTh) as a tetrahedral node to construct fully conjugated 3D COFs. The present work enriches the structural diversities and potential applications of 3D COFs.
M. Wu, Z. Shan, J. Wang, Z. Gu, X. Wu, B. Xu and G. Zhang, Chem. Commun., 2021, 57, 10379 DOI: 10.1039/D1CC03219D
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