A simple approach to a high sulfur-content material from biomass-derived guaiacol and waste sulfur is introduced. This direct reaction of elemental sulfur with an anisole derivative lacking olefins or halogen leaving groups expands the monomer scope beyond existing routes to high sulfur-content materials.
M. S. Karunarathna, M. K. Lauer and R. C. Smith, J. Mater. Chem. A, 2020, 8, 20318 DOI: 10.1039/D0TA07465A
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