The oxovanadium(V)-catalyzed oxidative cross-coupling of enolates using O2 as a terminal oxidant is reported, where a boron enolate and a silyl enol ether were employed as enolates. The redox behavior of V(V/IV) in this reaction under O2 was investigated by ESR and 51V NMR experiments.
Y. Osafune, Y. Jin, T. Hirao, M. Tobisu and T. Amaya, Chem. Commun., 2020, 56, 11697 DOI: 10.1039/D0CC04395H
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