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Scalable electrochemical oxidant-and metal-free dehydrogenative coupling of S–H/N–H

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Abstract

A practical and scalable electrochemical oxidation of S–H and N–H was developed. This oxidant- and catalyst-free electrochemical process enables S–N bond formation with inexpensive nickel electrodes in an undivided cell. This procedure exhibits broad substrate scopes and good functional-group compatibility. A 50 g scale oxidative coupling augurs well for industrial applications.

Graphical abstract: Scalable electrochemical oxidant-and metal-free dehydrogenative coupling of S–H/N–H

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Publication details

The article was received on 27 Dec 2018, accepted on 09 Jan 2019 and first published on 10 Jan 2019


Article type: Communication
DOI: 10.1039/C8OB03211D
Citation: Org. Biomol. Chem., 2019, Advance Article
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    Scalable electrochemical oxidant-and metal-free dehydrogenative coupling of S–H/N–H

    S. Tang, Y. Liu, L. Li, X. Ren, J. Li, G. Yang, H. Li and B. Yuan, Org. Biomol. Chem., 2019, Advance Article , DOI: 10.1039/C8OB03211D

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