Pore shape-reflecting morphosynthesis of lithium niobium oxide via mixed chloride flux growth in the presence of mesoporous silica

Minoru Sohmiya; Shinya Umehara; Shinpei Enomoto; Yusuke Ide; Tomohiko Okada; Yoshiyuki Sugahara; Makoto Ogawa

doi:10.1039/C9NA00097F

Pore shape-reflecting morphosynthesis of lithium niobium oxide via mixed chloride flux growth in the presence of mesoporous silica†

Minoru Sohmiya,

*^abc Shinya Umehara,^d Shinpei Enomoto,^c Yusuke Ide,

^de Tomohiko Okada,

^df Yoshiyuki Sugahara

^cdg and Makoto Ogawa

^bdh

Author affiliations

* Corresponding authors

^a Department of Materials and Life Science, Faculty of Science and Technology, Seikei University, 3-3-1 Kichijojikitamachi, Musashino-shi, Tokyo 180-8633, Japan
E-mail: minoru.sohmiya@st.seikei.ac.jp, minoru.sohmiya@gmail.com

^b Department of Earth Sciences, Waseda University, 1-6-1 Nishiwaseda, Shinjuku-ku, Tokyo 169-8050, Japan

^c Kagami Memorial Laboratory for Materials Science and Technology (Zaiken), Waseda University, 2-8-26 Nishiwaseda, Shinjuku-ku, Tokyo 169-0051, Japan

^d Graduate School of Creative Science and Engineering, Waseda University, 1-6-1 Nishiwaseda, Shinjuku-ku, Tokyo 169-8050, Japan

^e International Center for Materials Nanoarchitectonics (MANA), National Institute for Materials Science (NIMS), 1-1 Namiki, Tsukuba, Ibaraki 305-0044, Japan

^f Department of Chemistry and Materials Engineering, Faculty of Engineering, Shinshu University, 4-17-1 Wakasato, Nagano 380-8553, Japan

^g Department of Applied Chemistry, School of Advanced Science and Engineering, Waseda University, 3-4-1 Ohkubo, Shinjuku-ku, Tokyo 169-8555, Japan

^h School of Energy Science and Engineering, Vidyasirimedhi Institute of Science and Technology, 555 Moo 1, Payupnai, Wangchan, Rayong 21210, Thailand

Abstract

A new synthesis method, “chloride flux growth in the rigid nanospace of mesoporous silica”, was developed to obtain lithium niobium oxide anisotropic nanoparticles. The morphologies reflect the pore size and shape of the used mesoporous silicas. This method has great potential for synthesizing size-tuned anisotropic nanoparticles of other complex metal oxides.

Supplementary files

Article information

DOI: https://doi.org/10.1039/C9NA00097F
Article type: Communication
Submitted: 18 Feb 2019
Accepted: 09 Apr 2019
First published: 10 Apr 2019
This article is Open Access

Download Citation

Nanoscale Adv., 2019,1, 1726-1730

Permissions

Request permissions

Pore shape-reflecting morphosynthesis of lithium niobium oxide via mixed chloride flux growth in the presence of mesoporous silica

M. Sohmiya, S. Umehara, S. Enomoto, Y. Ide, T. Okada, Y. Sugahara and M. Ogawa, Nanoscale Adv., 2019, 1, 1726 DOI: 10.1039/C9NA00097F

This article is licensed under a Creative Commons Attribution 3.0 Unported Licence. You can use material from this article in other publications without requesting further permissions from the RSC, provided that the correct acknowledgement is given.

Nanoscale Advances

Pore shape-reflecting morphosynthesis of lithium niobium oxide via mixed chloride flux growth in the presence of mesoporous silica†

Abstract

Supplementary files

Article information

Download Citation

Permissions

Pore shape-reflecting morphosynthesis of lithium niobium oxide via mixed chloride flux growth in the presence of mesoporous silica

Social activity

Search articles by author

Spotlight

Advertisements