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Issue 11, 2019
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Solvent-free anhydrous Li+, Na+ and K+ salts of [B(3,5-(CF3)2C6H3)4], [BArF4]. Improved synthesis and solid-state structures

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Abstract

A modified, convenient, preparation of solvent-free, anhydrous, Li+, Na+ and K+ salts of the ubiquitous [BArF4] anion is reported, that involves a simple additional recrystallisation step. Anhydrous Na[BArF4], K[BArF4], and [Li(H2O)][BArF4], were characterised by single-crystal X-ray diffraction.

Graphical abstract: Solvent-free anhydrous Li+, Na+ and K+ salts of [B(3,5-(CF3)2C6H3)4]−, [BArF4]−. Improved synthesis and solid-state structures

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Publication details

The article was received on 17 Jan 2019, accepted on 30 Jan 2019 and first published on 14 Feb 2019


Article type: Communication
DOI: 10.1039/C9DT00235A
Citation: Dalton Trans., 2019,48, 3551-3554
  • Open access: Creative Commons BY license
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    Solvent-free anhydrous Li+, Na+ and K+ salts of [B(3,5-(CF3)2C6H3)4], [BArF4]. Improved synthesis and solid-state structures

    A. J. Martínez-Martínez and A. S. Weller, Dalton Trans., 2019, 48, 3551
    DOI: 10.1039/C9DT00235A

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