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Microwave-assisted synthesis of organically functionalized hexa-molybdovanadates

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Abstract

The microwave-assisted reaction of (TBA)4[β-Mo8O24] and (TBA)3[H3V10O28] with pentaerythritol or tris(hydroxymethyl)aminomethane yields polyanions with the general formula (TBA)2[V3Mo3O16(O3–R)] (R: C5H8OH – 1; R: C4H6NH23). Post-synthetic esterification of 1 yields the acylated derivative 2, with all compounds being characterized in the solid and solution state.

Graphical abstract: Microwave-assisted synthesis of organically functionalized hexa-molybdovanadates

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Article information


Submitted
01 Aug 2017
Accepted
15 Nov 2017
First published
08 Dec 2017

This article is Open Access

New J. Chem., 2018,42, 25-28
Article type
Letter

Microwave-assisted synthesis of organically functionalized hexa-molybdovanadates

H. Karoui and C. Ritchie, New J. Chem., 2018, 42, 25
DOI: 10.1039/C7NJ02820B

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