An efficient method for the catalytic deoxydehydration of renewable triols, including those obtained from 5-HMF, is described. The corresponding unsaturated alcohols were obtained in good yields using simple rhenium(VII)oxide under neat conditions and ambient atmosphere at 165 °C.
B. Wozniak, Y. Li, S. Tin and J. G. de Vries, Green Chem., 2018, 20, 4433 DOI: 10.1039/C8GC02387E
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