A simple, practical and governable palladium-catalyzed hydroformylation of terminal arylacetylenes has been disclosed. The reaction proceeds under syngas-free conditions, using readily available glyoxylic acid as the formyl source, under mild conditions, giving rise to a broad range of α,β-unsaturated aldehydes.
Y. Liu, L. Cai, S. Xu, W. Pu and X. Tao, Chem. Commun., 2018, 54, 2166 DOI: 10.1039/C7CC09629A
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