By using iridium catalysed dehydrogenative decarbonylation, we converted a partly protected cellobioside into a fully protected xylobioside. We demonstrate good yields with two different aromatic ester protecting groups. The resulting xylobioside was directly used as glycosyl donor in further synthesis of a xylooctaose.
M. J. Pedersen, R. Madsen and M. H. Clausen, Chem. Commun., 2018, 54, 952 DOI: 10.1039/C7CC09260A
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