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Issue 5, 2017
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Atom economical synthesis of N-alkylbenzamides via the iron(iii) sulfate catalyzed rearrangement of 2-alkyl-3-aryloxaziridines in water and in the presence of a surfactant

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Abstract

A green and mild synthetic route to N-alkylbenzamides involves eco-friendly one pot synthesis of 2-alkyl-3-aryloxaziridines from N-alkylamines and benzaldehydes followed by iron(III) sulfate catalyzed rearrangement to the corresponding amides in water as the solvent and in the presence of sodium dodecyl sulfate as the surfactant. This green approach affords N-alkylbenzamides in high overall yields under simple and minimum manipulation.

Graphical abstract: Atom economical synthesis of N-alkylbenzamides via the iron(iii) sulfate catalyzed rearrangement of 2-alkyl-3-aryloxaziridines in water and in the presence of a surfactant

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Article information


Submitted
27 Dec 2016
Accepted
21 Jan 2017
First published
23 Jan 2017

Green Chem., 2017,19, 1263-1267
Article type
Communication

Atom economical synthesis of N-alkylbenzamides via the iron(III) sulfate catalyzed rearrangement of 2-alkyl-3-aryloxaziridines in water and in the presence of a surfactant

J. Kraïem and T. Ollevier, Green Chem., 2017, 19, 1263
DOI: 10.1039/C6GC03589B

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