The synthesis of high surface-area colloidal assemblies of calixarene-phosphine-capped nanoporous gold is reported under reductive electrochemical conditions. These materials uniquely exhibit a remarkably thin wall thickness down to 10 nm, while possessing pore sizes on the order of up to hundreds of nanometers, which can be controlled via choice of organic ligand.
C. Schöttle, E. L. Clark, A. Harker, A. Solovyov, A. T. Bell and A. Katz, Chem. Commun., 2017, 53, 10870 DOI: 10.1039/C7CC05116F
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