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Abstract | Cited by

A Rh(III)-catalyzed C–H activation followed by conjugate addition to maleimides, using carboxylic acid as a traceless/deciduous directing group, to formally furnish a Csp2–Csp3 bond is presented. For the first time, derivatives of acrylic acid have been shown as surrogates for the unstable and expensive alkenyl boronic acids.

Graphical abstract: A deciduous directing group approach for the addition of aryl and vinyl nucleophiles to maleimides

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