Solvent-free on-surface synthesis of boroxine COF monolayers

Saskia Spitzer; Atena Rastgoo-Lahrood; Klaus Macknapp; Viktoria Ritter; Stefan Sotier; Wolfgang M. Heckl; Markus Lackinger

doi:10.1039/C7CC01131H

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Solvent-free on-surface synthesis of boroxine COF monolayers†

Saskia Spitzer,^ab Atena Rastgoo-Lahrood,^ab Klaus Macknapp,^a Viktoria Ritter,^b Stefan Sotier,^a Wolfgang M. Heckl^ab and Markus Lackinger

*^ab

Author affiliations

* Corresponding authors

^a Deutsches Museum, Museumsinsel 1, Munich, Germany

^b Department of Physics, Technische Universität München, James-Franck-Str. 1, Garching, Germany
E-mail: markus@lackinger.org

Abstract

A protocol is proposed for the solvent-free on-surface synthesis of covalent organic framework monolayers by condensation of diboronic acids. Monomers are vapor-deposited and water is used for equilibrium regulation. Samples are characterized on progressively smaller length scales by light microscopy, Scanning Electron Microscopy, and Scanning Tunneling Microscopy.

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Article information

DOI: https://doi.org/10.1039/C7CC01131H
Article type: Communication
Submitted: 13 Feb 2017
Accepted: 11 Apr 2017
First published: 12 Apr 2017

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Chem. Commun., 2017,53, 5147-5150

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Solvent-free on-surface synthesis of boroxine COF monolayers

S. Spitzer, A. Rastgoo-Lahrood, K. Macknapp, V. Ritter, S. Sotier, W. M. Heckl and M. Lackinger, Chem. Commun., 2017, 53, 5147 DOI: 10.1039/C7CC01131H

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Chemical Communications

Solvent-free on-surface synthesis of boroxine COF monolayers†

Abstract

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Solvent-free on-surface synthesis of boroxine COF monolayers

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