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Issue 7, 2015
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One-pot vinylogous aldol addition of β,γ-unsaturated esters under mild conditions

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Abstract

We described a one-pot vinylogous aldol addition of methyl 3-butenoate to aromatic aldehydes in the presence of silver salts and the TMSCl–TBAF mixture. The reaction can be done simply by sequentially mixing reagents in situ, and it does not require any catalyst or dienolate ether preparations prior to the reaction.

Graphical abstract: One-pot vinylogous aldol addition of β,γ-unsaturated esters under mild conditions

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Supplementary files

Article information


Submitted
17 Apr 2015
Accepted
22 May 2015
First published
22 May 2015

New J. Chem., 2015,39, 5121-5123
Article type
Letter
Author version available

One-pot vinylogous aldol addition of β,γ-unsaturated esters under mild conditions

İ. Akçok and A. Çağır, New J. Chem., 2015, 39, 5121 DOI: 10.1039/C5NJ00961H

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