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Issue 28, 2015
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Double [3 + 2]-dimerisation cascade synthesis of bis(triazolyl)bisphosphanes, a new scaffold for bidentate bisphosphanes

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Abstract

A highly convergent synthesis of bis(triazolylphosphane oxides) was developed by a tandem copper-mediated Huisgen reaction–oxidative coupling. The phosphane oxides were reduced by trichlorosilane and the coordination of the resulting bisphosphanes was studied with various transition metals.

Graphical abstract: Double [3 + 2]-dimerisation cascade synthesis of bis(triazolyl)bisphosphanes, a new scaffold for bidentate bisphosphanes

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Publication details

The article was received on 09 Jun 2015, accepted on 16 Jun 2015 and first published on 16 Jun 2015


Article type: Communication
DOI: 10.1039/C5DT02197A
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Citation: Dalton Trans., 2015,44, 12539-12545
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    Double [3 + 2]-dimerisation cascade synthesis of bis(triazolyl)bisphosphanes, a new scaffold for bidentate bisphosphanes

    C. Laborde, M. Wei, A. van der Lee, E. Deydier, J. Daran, J. Volle, R. Poli, J. Pirat, E. Manoury and D. Virieux, Dalton Trans., 2015, 44, 12539
    DOI: 10.1039/C5DT02197A

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