A huge diamondoid metal–organic framework featuring a tenfold interpenetrating neo-mode, with an extra-framework volume of up to 48.7% despite its very high degree of interpenetration, is reported. The hydrogen bonding of the inter-networks directs the relative position of the frameworks and exhibits a self-catenated net with a point symbol of {(62.84)(64.8.10)2}.
T. Tseng, T. Luo, C. Tsai and K. Lu, CrystEngComm, 2015, 17, 2935 DOI: 10.1039/C5CE00037H
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