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Issue 104, 2014
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Convenient synthesis of α-nitrooximes mediated by OXONE®

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Abstract

A novel OXONE® mediated direct difunctionalization of alkenes with NaNO2 in aqueous acetonitrile for the synthesis of α-nitrooximes was developed. The α-nitrooximes were readily prepared in moderate to high yields at room temperature under mild reaction conditions. The present protocol offers an easy and environmentally benign approach to access various α-nitrooximes derived from styrene derivatives.

Graphical abstract: Convenient synthesis of α-nitrooximes mediated by OXONE®

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Publication details

The article was received on 03 Oct 2014, accepted on 28 Oct 2014 and first published on 28 Oct 2014


Article type: Paper
DOI: 10.1039/C4RA11703D
Citation: RSC Adv., 2014,4, 59726-59732
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    Convenient synthesis of α-nitrooximes mediated by OXONE®

    N. Chumnanvej, N. Samakkanad, M. Pohmakotr, V. Reutrakul, T. Jaipetch, D. Soorukram and C. Kuhakarn, RSC Adv., 2014, 4, 59726
    DOI: 10.1039/C4RA11703D

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