A simple and efficient method for the synthesis of pyranoid glycals utilizing the reductive elimination of glycopyranosyl bromides by zinc nanoparticles in an acetate buffer is described. A variety of pyranoid glycals derivatives were obtained, especially for the synthesis of 6-deoxy-4,6-O-benzylidene and disaccharide glycals with good yields.
Y. Xu, W. Wang, Y. Cai, X. Yang, P. G. Wang and W. Zhao, RSC Adv., 2014, 4, 46662 DOI: 10.1039/C4RA08028A
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