The M(II)/M(III) ratio is an important structural feature of layered double hydroxides (LDHs). Here, we report a convenient chemical titration method to measure the M(II)/M(III) ratio of LDHs. The measured results have a relative standard deviation of less than 1.0%, and agree with the data measured by inductively coupled plasma (ICP) atomic emission spectroscopy very well.
Z. Zhang and G. Chen, RSC Adv., 2014, 4, 31333 DOI: 10.1039/C4RA04273E
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