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Issue 1, 2014
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Quantification of ion binding using electrospray mass spectrometry

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Abstract

Mass spectrometry has predominately been used as a qualitative tool in the analysis of complexes with quantitative studies being difficult to validate. Here, we present a method where electrospray mass spectrometry is used to give both a qualitative and quantitative measure of ion binding with cross validation by solution 1H NMR, demonstrating it is possible to utilize gas-phase electrospray mass spectrometry continuous variation data to deduce binding stoichiometries in solutions where artifacts and nonspecific complexes are also observed.

Graphical abstract: Quantification of ion binding using electrospray mass spectrometry

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Supplementary files

Article information


Submitted
10 Sep 2013
Accepted
23 Oct 2013
First published
06 Jan 2014

Inorg. Chem. Front., 2014,1, 49-52
Article type
Communication

Quantification of ion binding using electrospray mass spectrometry

J. S. Mathieson, G. J. T. Cooper, M. D. Symes and L. Cronin, Inorg. Chem. Front., 2014, 1, 49
DOI: 10.1039/C3QI00037K

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