Issue 5, 2014
From the journal:

Green Chemistry

Metal-free cross-coupling reaction of aldehydes with disulfides by using DTBP as an oxidant under solvent-free conditions†

Jing-Wen Zeng,a   Yi-Chen Liu,a   Ping-An Hsieh,a   Yu-Ting Huang,a   Chih-Lun Yi,a   Satpal Singh Badsaraa  and  Chin-Fa Lee*a  

* Corresponding authors

a Department of Chemistry, National Chung Hsing University, Taichung, Taiwan 402, Republic of China
E-mail: cfalee@dragon.nchu.edu.tw
Fax: (+886) 4-2286-2547
Tel: +886 4 2284-0411 ext. 810

Abstract

A DTBP-promoted C–H thiolation of aldehydes with disulfides under metal-free and solvent-free conditions is described. The system shows good functional group tolerance to afford thioesters in moderate to excellent yields.

Graphical abstract: Metal-free cross-coupling reaction of aldehydes with disulfides by using DTBP as an oxidant under solvent-free conditions

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Article information

DOI
https://doi.org/10.1039/C4GC00025K
Article type
Paper
Submitted
07 Jan 2014
Accepted
06 Feb 2014
First published
10 Feb 2014

Green Chem., 2014,16, 2644-2652

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Metal-free cross-coupling reaction of aldehydes with disulfides by using DTBP as an oxidant under solvent-free conditions

J. Zeng, Y. Liu, P. Hsieh, Y. Huang, C. Yi, S. S. Badsara and C. Lee, Green Chem., 2014, 16, 2644 DOI: 10.1039/C4GC00025K

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