Extensive solid-state NMR analyses unambiguously determine the formation of silica supported W bis-methylidene methyl species by reaction of the corresponding methyl carbyne with trimethylphosphine or a cyclic olefin.
E. Callens, E. Abou-Hamad, N. Riache and J. M. Basset, Chem. Commun., 2014, 50, 3982 DOI: 10.1039/C4CC00286E
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