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Issue 3, 2013
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Probing self-assembled 1,3,5-benzenetrisamides in isotactic polypropylene by 13C DQ solid-state NMR spectroscopy

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Abstract

Using 13C double quantum solid-state NMR spectroscopy, we were able to observe nuclei of a supramolecular BTA based additive on the nanoscale in a matrix of i-PP at a concentration of only 0.09 wt%. These nuclei exhibit the analogous structural features as the crystalline phase of the neat additive.

Graphical abstract: Probing self-assembled 1,3,5-benzenetrisamides in isotactic polypropylene by 13C DQ solid-state NMR spectroscopy

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Article information


Submitted
16 Aug 2012
Accepted
08 Nov 2012
First published
22 Nov 2012

Chem. Commun., 2013,49, 267-269
Article type
Communication

Probing self-assembled 1,3,5-benzenetrisamides in isotactic polypropylene by 13C DQ solid-state NMR spectroscopy

M. Schmidt, J. J. Wittmann, R. Kress, H. Schmidt and J. Senker, Chem. Commun., 2013, 49, 267
DOI: 10.1039/C2CC37384J

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