Issue 3, 2013

Probing self-assembled 1,3,5-benzenetrisamides in isotactic polypropylene by 13C DQ solid-state NMR spectroscopy

Abstract

Using 13C double quantum solid-state NMR spectroscopy, we were able to observe nuclei of a supramolecular BTA based additive on the nanoscale in a matrix of i-PP at a concentration of only 0.09 wt%. These nuclei exhibit the analogous structural features as the crystalline phase of the neat additive.

Graphical abstract: Probing self-assembled 1,3,5-benzenetrisamides in isotactic polypropylene by 13C DQ solid-state NMR spectroscopy

Supplementary files

Article information

Article type
Communication
Submitted
16 Aug 2012
Accepted
08 Nov 2012
First published
22 Nov 2012

Chem. Commun., 2013,49, 267-269

Probing self-assembled 1,3,5-benzenetrisamides in isotactic polypropylene by 13C DQ solid-state NMR spectroscopy

M. Schmidt, J. J. Wittmann, R. Kress, H. Schmidt and J. Senker, Chem. Commun., 2013, 49, 267 DOI: 10.1039/C2CC37384J

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