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Issue 33, 2012
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Trichloroisocyanuric acid (TCCA)–TMSOTf: an efficient activator system for glycosylation reactions based on thioglycosides

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Abstract

Trichloroisocyanuric acid (TCCA), a readily available, inexpensive and shelf-stable reagent, in combination with a catalytic amount of TMSOTf, has been used for the first time for efficient glycosylation reactions based on thioglycoside donors with SEt, SPh and S-pTol leaving groups at the anomeric centres.

Graphical abstract: Trichloroisocyanuric acid (TCCA)–TMSOTf: an efficient activator system for glycosylation reactions based on thioglycosides

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Publication details

The article was received on 17 Aug 2012, accepted on 11 Oct 2012 and first published on 12 Oct 2012


Article type: Communication
DOI: 10.1039/C2RA21851H
Citation: RSC Adv., 2012,2, 12661-12664

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    Trichloroisocyanuric acid (TCCA)–TMSOTf: an efficient activator system for glycosylation reactions based on thioglycosides

    N. Basu, S. Kumar Maity and R. Ghosh, RSC Adv., 2012, 2, 12661
    DOI: 10.1039/C2RA21851H

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