Radical-mediated reduction of the dithiocarbamate group under tin-free conditions†
Abstract
Reductive desulfurisation of dithiocarbamates is conveniently achieved using H3PO2–Et3N–ACCN in refluxing
* Corresponding authors
a
School of Chemistry, University of Birmingham, Edgbaston, Birmingham B15 2TT, UK
E-mail:
r.s.grainger@bham.ac.uk
Fax: +44 (0) 121 4144403
Tel: +44 (0) 121 4144465
b GlaxoSmithKline, Gunnels Wood Road, Stevenage, Herts SG1 2NY, UK
Reductive desulfurisation of dithiocarbamates is conveniently achieved using H3PO2–Et3N–ACCN in refluxing
C. McMaster, R. N. Bream and R. S. Grainger, Org. Biomol. Chem., 2012, 10, 4752 DOI: 10.1039/C2OB25434D
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