Issue 1, 2012
From the journal:

Green Chemistry

Development of a fluorous, oxime-based palladacycle for microwave-promoted carbon–carbon coupling reactions in aqueous media†

Woen Susanto,a   Chi-Yuan Chu,b   Wei Jie Ang,a   Tzyy-Chao Chou,b   Lee-Chiang Lo*b  and  Yulin Lam*a  

* Corresponding authors

a Department of Chemistry, National University of Singapore, 3 Science Drive 3, Singapore
E-mail: chmlamyl@nus.edu.sg
Fax: 65-67791691
Tel: 65-65162688

b Department of Chemistry, National Taiwan University, No. 1, Sec. 4 Roosevelt Road, Taipei, Taiwan
E-mail: lclo@ntu.edu.tw
Fax: 886-223636359
Tel: 886-233661669

Abstract

A thermally stable, fluorous oxime-based palladacycle has been developed and was shown to efficiently promote various carbon–carbon bond formation reactions (Suzuki–Miyaura, Sonogashira and Stille) in aqueous media under microwave irradiation. The palladacycle gave extremely low levels of Pd leaching and could be reused five times with no significant loss of activity.

Graphical abstract: Development of a fluorous, oxime-based palladacycle for microwave-promoted carbon–carbon coupling reactions in aqueous media

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Article information

DOI
https://doi.org/10.1039/C1GC16108C
Article type
Communication
Submitted
06 Sep 2011
Accepted
21 Oct 2011
First published
14 Nov 2011

Green Chem., 2012,14, 77-80

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Development of a fluorous, oxime-based palladacycle for microwave-promoted carbon–carbon coupling reactions in aqueous media

W. Susanto, C. Chu, W. J. Ang, T. Chou, L. Lo and Y. Lam, Green Chem., 2012, 14, 77 DOI: 10.1039/C1GC16108C

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