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Issue 4, 2012
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Palladium(II)–selenoether complexes as new single source precursors: First synthesis of Pd4Se and Pd7Se4 nanoparticles

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Abstract

Pd4Se and Pd7Se4 nanoparticles (size 38–104 nm), protected by TOP, have been obtained for the first time using Pd(II) ligated with selenated primary and secondary amines (see 1 and 2) as single source precursors respectively. TEM, SEM, powder XRD and photoluminescence have been used to characterize them. 1 and 2 are also the first Pd(II)–selenoether complexes used for the synthesis of nanoparticles containing palladium and selenium.

Graphical abstract: Palladium(ii)–selenoether complexes as new single source precursors: First synthesis of Pd4Se and Pd7Se4 nanoparticles

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Publication details

The article was received on 04 Nov 2011, accepted on 22 Nov 2011 and first published on 12 Dec 2011


Article type: Communication
DOI: 10.1039/C2DT12113A
Dalton Trans., 2012,41, 1142-1145

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    Palladium(II)–selenoether complexes as new single source precursors: First synthesis of Pd4Se and Pd7Se4 nanoparticles

    V. V. Singh, G. K. Rao, A. Kumar and A. K. Singh, Dalton Trans., 2012, 41, 1142
    DOI: 10.1039/C2DT12113A

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