Issue 2, 2012
From the journal:

CrystEngComm

Polymorphism of 4-tert-butylcalix[4]arene upon formation of n-hexane and acetonitrile complexes and thermal desolvation

Oleg V. Surov,*a   Marina I. Voronova,a   Pavel R. Smirnov,a   Nugzar Z. Mamardashvilia  and  Gennady P. Shaposhnikovb  

* Corresponding authors

a Institute of Solution Chemistry of the Russian Academy of Sciences, Akademicheskaya Str, 1, Ivanovo, Russia
E-mail: ovs@isc-ras.ru
Fax: +4932 336237
Tel: +4932 336990

b Ivanovo State University of Chemistry and Technology, F. Engels Avenue, 7, Ivanovo, Russia

Abstract

Simultaneous analysis of X-ray powder diffraction patterns and DSC traces for 4-tert-butylcalix[4]arene-n-hexane and 4-tert-butylcalix[4]arene-acetonitrile compounds as functions of thermal history allows us to reveal the complex relationship between guest-free polymorphic products and desolvation of 4-tert-butylcalix[4]arene inclusion compounds.

Graphical abstract: Polymorphism of 4-tert-butylcalix[4]arene upon formation of n-hexane and acetonitrile complexes and thermal desolvation

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Article information

DOI
https://doi.org/10.1039/C1CE05469D
Article type
Paper
Submitted
19 Apr 2011
Accepted
23 Sep 2011
First published
31 Oct 2011

CrystEngComm, 2012,14, 533-536

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Polymorphism of 4-tert-butylcalix[4]arene upon formation of n-hexane and acetonitrile complexes and thermal desolvation

O. V. Surov, M. I. Voronova, P. R. Smirnov, N. Z. Mamardashvili and G. P. Shaposhnikov, CrystEngComm, 2012, 14, 533 DOI: 10.1039/C1CE05469D

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