Iron-catalysed tandem cross-dehydrogenative coupling (CDC) of terminal allylic C(sp3) to C(sp2) of styrene and benzoannulation in the synthesis of polysubstituted naphthalenes

Hua Liu; Li Cao; Jia Sun; John S. Fossey; Wei-Ping Deng

doi:10.1039/C2CC17330A

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Iron-catalysed tandem cross-dehydrogenative coupling (CDC) of terminal allylic C(sp³) to C(sp²) of styrene and benzoannulation in the synthesis of polysubstituted naphthalenes†

Hua Liu,^a Li Cao,^a Jia Sun,^a John S. Fossey^ab and Wei-Ping Deng*^a

Author affiliations

* Corresponding authors

^a School of Pharmacy and Shanghai Key Laboratory of Functional Materials Chemistry, East China University of Science and Technology, 130 Meilong Road, Shanghai 200237, China
E-mail: weiping_deng@ecust.edu.cn

^b School of Chemistry, University of Birmingham, Edgbaston, Birmingham, UK
E-mail: j.s.fossey@bham.ac.uk

Abstract

A novel iron-catalysed tandem cross-dehydrogenative coupling and benzoannulation process was developed for the synthesis of biologically and synthetically important polysubstituted naphthalene derivatives from simple 1,2-aryl-propenes and styrenes in moderate to good yields.

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Article information

DOI: https://doi.org/10.1039/C2CC17330A
Article type: Communication
Submitted: 24 Nov 2011
Accepted: 12 Jan 2012
First published: 16 Jan 2012

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Chem. Commun., 2012,48, 2674-2676

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Iron-catalysed tandem cross-dehydrogenative coupling (CDC) of terminal allylic C(sp³) to C(sp²) of styrene and benzoannulation in the synthesis of polysubstituted naphthalenes

H. Liu, L. Cao, J. Sun, J. S. Fossey and W. Deng, Chem. Commun., 2012, 48, 2674 DOI: 10.1039/C2CC17330A

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