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In this work we demonstrated a facile method for in situ fabrication of the Fe3+–1,3,5-benzenetricarboxylic acid (BTC) metal–organic coordination polymer gel in a capillary, which was efficiently applied to the online enrichment of trace polycyclic aromatic hydrocarbons (PAHs) in environmental water and amphetamines drugs in urine.

Graphical abstract: In situ fabrication of metal–organic hybrid gels in a capillary for online enrichment of trace analytes in aqueous samples

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