A facile one-pot reflux method was explored for large-scale preparation of todorokite-type manganese oxide octahedral molecular sieves (OMS-1) composed of hierarchical nanoplate microspheres. The diameters of the microspheres are usually 1.5–2.5 μm, and the thickness of the nanoplate is approximately 10 nm.
H. Cui, J. Shi, F. Liu and M. Fu, J. Mater. Chem., 2011, 21, 18527 DOI: 10.1039/C1JM13964A
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