Issue 2, 2011
From the journal:

CrystEngComm

Solid-state assembly of calixcyclitol derivatives†

Carmine Gaeta,*ab   Francesco Troisi,a   Riccardo Spagna,c   Mercedes Camalli,c   Gaetano Campic  and  Placido Neri*ab  

* Corresponding authors

a Dipartimento di Chimica, Università di Salerno, Via Ponte don Melillo, Fisciano, Salerno, Italy
E-mail: cgaeta@unisa.it, neri@unisa.it
Fax: +39089969603
Tel: +39089969556

b NANO_MATES, Research Centre for NANOMAterials and nanoTEchnology at Salerno University, Università di Salerno, Via Ponte don Melillo, Fisciano, SA, Italy

c Istituto di Cristallografia-Sezione di Monterotondo, CNR, Area della Ricerca Roma 1, C.P. n.10, Monterotondo Stazione, Roma, Italy

Abstract

The solid-state assembly of two calixcyclitol derivatives bearing two or one rings (compounds 1 or 2, respectively) oxyfunctionalized with oxetane and hydroxyl functional groups has been structurally studied by X-ray crystallography. Calixcyclitol 1 can assemble to give a H-bonded layered (crystals 1A) or double-columnar (crystals 1B) structure with alternating polar and lipophilic zones. Calixcyclitol 2 gives a double-helical arrangement through the intermediacy of H2O and MeOH molecules.

Graphical abstract: Solid-state assembly of calixcyclitol derivatives

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Article information

DOI
https://doi.org/10.1039/C0CE00099J
Article type
Paper
Submitted
15 Apr 2010
Accepted
12 Jul 2010
First published
08 Sep 2010

CrystEngComm, 2011,13, 467-473

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Solid-state assembly of calixcyclitol derivatives

C. Gaeta, F. Troisi, R. Spagna, M. Camalli, G. Campi and P. Neri, CrystEngComm, 2011, 13, 467 DOI: 10.1039/C0CE00099J

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