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Issue 3, 2011
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Intramolecular iodoetherification of ene or diene ketals: facile synthesis of spiroketals

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Abstract

A novel and rapid approach to chiral mono- or di-substituted spiroketals based on remote asymmetric induction by intramolecular iodoetherification of ene or diene ketals has been developed. This strategy concisely offers 5,5- and 5,6-spiroketals including the natural insect pheromone of the wasp.

Graphical abstract: Intramolecular iodoetherification of ene or diene ketals: facile synthesis of spiroketals

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Article information


Submitted
17 Sep 2010
Accepted
27 Oct 2010
First published
15 Nov 2010

Chem. Commun., 2011,47, 1060-1062
Article type
Communication

Intramolecular iodoetherification of ene or diene ketals: facile synthesis of spiroketals

H. Fujioka, K. Nakahara, H. Hirose, K. Hirano, T. Oki and Y. Kita, Chem. Commun., 2011, 47, 1060
DOI: 10.1039/C0CC03933K

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