Issue 12, 2011
From the journal:

Chemical Communications

Syntheses and structures of triazides of heavy group 15 elements†

Stephan Schulz,*a   Benjamin Lyhs,a   Georg Jansen,a   Dieter Bläsera  and  Christoph Wölpera  

* Corresponding authors

a University of Duisburg-Essen, Universitätsstr. 5-7, S07 S03 C30, 45117 Essen, Germany
E-mail: stephan.schulz@uni-due.de
Fax: +49 201 1833830
Tel: +49 201 1834635

Abstract

Synthesis of group 15-triazides E(N3)3 (E = Sb 1, Bi 2) and Py2–Bi(N3)33 (Py = pyridine). Single crystals of 1 were in situ grown by an IR-laser-assisted technique on the diffractometer. The structure of 3, which represents the first structurally characterized neutral Bi-triazide, is influenced by crystal packing effects according to DFT calculations.

Graphical abstract: Syntheses and structures of triazides of heavy group 15 elements

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Article information

DOI
https://doi.org/10.1039/C1CC10237K
Article type
Communication
Submitted
13 Jan 2011
Accepted
03 Feb 2011
First published
18 Feb 2011

Chem. Commun., 2011,47, 3401-3403

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Syntheses and structures of triazides of heavy group 15 elements

S. Schulz, B. Lyhs, G. Jansen, D. Bläser and C. Wölper, Chem. Commun., 2011, 47, 3401 DOI: 10.1039/C1CC10237K

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