Issue 17, 2011
From the journal:

Chemical Communications

Synthesis of a spirobifluorene-bridged allylsilane precursor for periodic mesoporous organosilica†

Natsuko Tanaka,a   Norihiro Mizoshita,bc   Yoshifumi Maegawa,bc   Takao Tani,bc   Shinji Inagaki,*bc   Yogesh R. Jorapurac  and  Toyoshi Shimada*ac  

* Corresponding authors

a Department of Chemical Engineering, Nara National College of Technology, 22 Yata-cho, Yamatokoriyama, Nara 639-1080, Japan
E-mail: shimada@chem.nara-k.ac.jp
Fax: +81-743-55-6154
Tel: +81-743-55-6154

b Toyota Central R&D Laboratories Inc., Nagakute, Aichi 480-1192, Japan
E-mail: inagaki@mosk.tytlabs.co.jp
Fax: +81-561-63-6507
Tel: +81-561-71-7393

c Core Research for Evolutional Science and Technology (CREST), Japan Science and Technology Agency (JST), Kawaguchi, Saitama 332-0012, Japan

Abstract

A novel spirobifluorene-bridged allylsilane precursor, which can be easily purified by silica gel chromatography, was prepared by using a new molecular building block for allylsilane sol–gel precursors (MBAS) and successfully converted into a highly fluorescent periodic mesoporous organosilica film.

Graphical abstract: Synthesis of a spirobifluorene-bridged allylsilane precursor for periodic mesoporous organosilica

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Article information

DOI
https://doi.org/10.1039/C0CC05823H
Article type
Communication
Submitted
28 Dec 2010
Accepted
05 Mar 2011
First published
24 Mar 2011

Chem. Commun., 2011,47, 5025-5027

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Synthesis of a spirobifluorene-bridged allylsilane precursor for periodic mesoporous organosilica

N. Tanaka, N. Mizoshita, Y. Maegawa, T. Tani, S. Inagaki, Y. R. Jorapur and T. Shimada, Chem. Commun., 2011, 47, 5025 DOI: 10.1039/C0CC05823H

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