Issue 11, 2011
From the journal:

Chemical Communications

A new and general one-pot synthesis of propargyl alcohols from esters

Min Jung Chae,a   Ah Ram Jeon,a   Tom Livinghouseb  and  Duk Keun An*a  

* Corresponding authors

a Department of Chemistry, Kangwon National University, and Institute for Molecular Science and Fusion Technology, Chuncheon 200-701, Korea
E-mail: dkan@kangwon.ac.kr
Fax: +82 33-253-7582
Tel: +82 33-250-8494

b Department of Chemistry and Biochemistry, Montana State University, Bozeman, MT 59715, USA

Abstract

Intermediates easily prepared by partial reduction of various esters with LDBBA as a reducing agent smoothly react with lithium acetylides to give propargyl alcohols, without isolation of partial reduction intermediates, in good yields (73–83%).

Graphical abstract: A new and general one-pot synthesis of propargyl alcohols from esters

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Article information

DOI
https://doi.org/10.1039/C0CC04597G
Article type
Communication
Submitted
25 Oct 2010
Accepted
05 Jan 2011
First published
01 Feb 2011

Chem. Commun., 2011,47, 3281-3283

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A new and general one-pot synthesis of propargyl alcohols from esters

M. J. Chae, A. R. Jeon, T. Livinghouse and D. K. An, Chem. Commun., 2011, 47, 3281 DOI: 10.1039/C0CC04597G

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