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Issue 23, 2010
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Preparation of arylsulfonyl chlorides by chlorosulfonylation of in situ generated diazonium salts using a continuous flow reactor

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Abstract

A new flow procedure for the preparation of arylsulfonyl chlorides from aniline starting materials is described. The reaction conditions are mild, requiring no added acid and are amenable to continuous flow processing, in a safe, easily scalable and less labour intensive way than the corresponding batch method.

Graphical abstract: Preparation of arylsulfonyl chlorides by chlorosulfonylation of in situ generated diazonium salts using a continuous flow reactor

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Publication details

The article was received on 19 Jul 2010, accepted on 27 Aug 2010 and first published on 27 Sep 2010


Article type: Paper
DOI: 10.1039/C0OB00450B
Citation: Org. Biomol. Chem., 2010,8, 5324-5332

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    Preparation of arylsulfonyl chlorides by chlorosulfonylation of in situ generated diazonium salts using a continuous flow reactor

    L. Malet-Sanz, J. Madrzak, S. V. Ley and I. R. Baxendale, Org. Biomol. Chem., 2010, 8, 5324
    DOI: 10.1039/C0OB00450B

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