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Issue 40, 2010
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Direct structure elucidation by powder X-ray diffraction of a metal–organic framework material prepared by solvent-free grinding

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Abstract

Powder X-ray diffraction (XRD) has been exploited to establish the structural properties of a porous interpenetrated mixed-ligand metal–organic framework material prepared by solid-state grinding, recognizing that product phases from mechanochemical synthesis are typically microcrystalline powders. The importance of subjecting the powder XRD data to rigorous scrutiny in such applications is emphasized.

Graphical abstract: Direct structure elucidation by powder X-ray diffraction of a metal–organic framework material prepared by solvent-free grinding

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Publication details

The article was received on 17 Jul 2010, accepted on 27 Aug 2010 and first published on 17 Sep 2010


Article type: Communication
DOI: 10.1039/C0CC02635B
Citation: Chem. Commun., 2010,46, 7572-7574
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    Direct structure elucidation by powder X-ray diffraction of a metal–organic framework material prepared by solvent-free grinding

    K. Fujii, A. L. Garay, J. Hill, E. Sbircea, Z. Pan, M. Xu, D. C. Apperley, S. L. James and K. D. M. Harris, Chem. Commun., 2010, 46, 7572
    DOI: 10.1039/C0CC02635B

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